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See Latest ArticlesHomicide involving Aconitum tuberous root: LC-MS-MS analysis of Aconitum alkaloids and their hydrolysates in formalin-fixed tissues
Forensic Toxicology, 08/10/09
Miyaguchi H et al. – The authors describe a homicide case involving Aconitum tuberous roots, in which formalin–fixed solid tissues were analyzed for diester–type Aconitum alkaloids and their hydrolysates by liquid chromatography–tandem mass spectrometry. This procedure allowed detection of 0.10 ng/g for each of the spiked alkaloids from the formalin–fixed liver by quadrupole LC–MS–MS, and 10 pg/g for benzoylaconine and benzoylmesaconine by ion–trap LC–MS–MS. Sub–parts–per–billion levels of benzoylaconine and benzoylmesaconine could be detected from the formalin–fixed liver, kidney, and lung specimens.
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